By D E Hathway
Expert Periodical reviews supply systematic and distinctive overview assurance of development within the significant parts of chemical learn. Written by way of specialists of their expert fields the sequence creates a special provider for the lively study chemist, delivering normal serious in-depth debts of development particularly components of chemistry. For over eighty years the Royal Society of Chemistry and its predecessor, the Chemical Society, were publishing reviews charting advancements in chemistry, which initially took the shape of Annual studies. in spite of the fact that, by way of 1967 the complete spectrum of chemistry may well n learn more... summary: expert Periodical stories offer systematic and particular assessment insurance of growth within the significant components of chemical examine. Written by way of specialists of their expert fields the sequence creates a different provider for the energetic study chemist, delivering normal severe in-depth debts of development particularly parts of chemistry. For over eighty years the Royal Society of Chemistry and its predecessor, the Chemical Society, were publishing reviews charting advancements in chemistry, which initially took the shape of Annual studies. besides the fact that, via 1967 the complete spectrum of chemistry may possibly n
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Extra resources for Foreign Compound Metabolism in Mammals Volume 2
1971, 60, 1589. 7O The tritiated form was obtained by exchange with tritiated acetic acid, whereas [1-14C]naphth-l-ol was the precursor in the synthetic sequence indicated (Scheme 26). 'l The synthetic scheme is outlined below (Scheme 27). The related (59) has been labelled carcinogen N-hydroxy-2-fluorenylbenzenesulphonate m (57) Scheme 27 'O 'l J. Burns, J . Labelled Compounds, 1970, 6, 45. Nguyen-Hoang-Nam, H. Hoellinger, M. Herbert, Nguyen-Dat-Xuong, and L. Pichat, J. Labelled Compounds, 1970, 6, 99.
O 1 W. Michaelis, J. H. Russel, and 0. Schindler, J. Medicin. , 1970, 13, 497. at T. Meshi, M. Yoshikawa, and Y . Sato, Biochem. , 1970,19, 1351. (OH)Ph (43) Scheme 18 n (4541 (451 whereas the corresponding [36S]sulphonewas obtained by hydrogen peroxide oxidation of bithionol sulphoxide. 3,5-Dichloro-2-hydroxyphenylsulphonic acid was prepared from chloro [35S]sulphonicacid. Catalytic hydrogenation of bithionol sulphone in the presence of tritium gas gave C3H]bi s-(2-hydroxypheny1)sulphone. 3-Methyl-4- [ 4C]meth ylphenyl N-methylcarbamate (46) ([ 4C]Meobal) has been prepared from [14C]methyliodide as starting Alkylation of 3-methyl-4-lithioanisole(47), followed by cleavage of the methyl ether and reaction of the resultant phenol with methyl isocyanate, afforded the product.
Ph - M g- E t70 - \/I ’ Me Ph\ ’H &Me1 M ‘e si/ Me Mg -Et20 *Me1 ‘cr * * PhSiHMez Scheme 7 Radiocarbon- and tritium-labelled forms of Cardison, DL-N-methyl-Npropargyl-1-phenyl-Zaminopropanehydrochloride (13), have been prepared, and their syntheses described in A key intermediate, DL-N-methylphenylisopropylamine(14),was obtained by reductive condensationof phenylacetone and methylamine in the presence of sodium borohydride. Phenyl[2-14C]acetone and phenyl [3-14C]acetonewere obtained from the appropriately labelled ethyl acetates by the method indicated (Scheme 8).