Advanced inorganic chemistry, 6th Edition by Cotton F., Wilkinson G., Murillo C., Bochmann M.

By Cotton F., Wilkinson G., Murillo C., Bochmann M.

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Figure 4. Rh4(CO)12 cluster conversion into acyl-metal intermediate As reported in the same paper, it is likely that this unstable rhodium cluster is converted into the mononuclear rhodium-hydride species HRh(CO)x (x = 3,4), which are usually considered as the true catalyst system in the reaction mixture. These compounds represent extremely unstable intermediates, which would certainly recombine to form higher nuclearity rhodium species if alkene is not present in the reaction mixture. This mechanism is proposed for all the hydroformylation experiments carried out in the presence of Rh4(CO)12.

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