Acronyms and Abbreviations in Molecular Spectroscopy: An by Detlef A.W. Wendisch

By Detlef A.W. Wendisch

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Magn. Reson. 57: 331 2. Kessler H, Bermel W, Griesinger C (1985) 1. Am. Chern. Soc. 107: 1083 3. Kessler H, Griesinger C, Lautz 1 (1984) Angew. Chern. Int. Ed. Eng!. 23: 444 C -- 50 COLOC-S 4. Aue WP, Karhan J, Ernst RR (1976) J. Chern. Phys. 64: 4226 5. Wagner G, Wuthrich K, Tschesche H (1978) Eur. J. Biochern. 86: 67 COLOC-S Acronym for a modified COLOC experiment (see COLOC), where S stands for Selective The original COLOC experiment of Kessler and co-workers [1] modifies the basic C-H correlation sequence by introducing 180 pulses which are stepped incrementally through a fixed proton-evolution time, thus effecting broad-band decoupling (see BB) in the F 1 frequency domain.

References 1. Hosur RV, Ravikumar M, Sheth A (1985) J. Magn. Reson. 65: 375 2. 3. 4. 5. Bax A, Freeman R (1981) J. Magn. Reson. 44: 542 Rance M, Wagner G, SI'Jrensen OW, Wiithrich K, Ernst RR (1984) J. Magn. Reson. 59: 250 Hosur RV, Sheth A, Majumdar A (1988) J. Magn. Reson. 76: 218 SI'Jrensen OW, Eich GW, Levitt MH, Bodenhausen G, Ernst RR (1983) Prog. NMR Spectrosc.

Recently BIRD has been used for sensitivity-enhanced two-dimensional heteronuclear shift correlation NMR spectroscopy (see COSY) in the following way [4]: All protons not coupled to carbon-13 (low-y nucleus) are inverted by the BIRD pulse sequence [1,2]: 90~ eH)-1/(2J) -180~ eH, 13C)-1/(2J)-90~x e H), where J is the onebond 13C_1H-scalar coupling constant. Protons coupled to 13C are not affected by this bilinear pulse, whereas the magnetization of all other protons is inverted. e. when protons not coupled to carbon-13 are nearly saturated), the first 90° pulse of a heteronuclear multiple-quantum coherence (see HMQc) experiment is applied.

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